Synthesis and Hydrolysis Monitoring of Sasrin-like Resin Bound Imines by Fluorescence Spectroscopy
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| Format: | Artículo científico |
| Language: | en |
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Sociedad Química de México
2006
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| author | Domingo Madrigal |
| author_facet | Domingo Madrigal |
| contents | Synthesis and Hydrolysis Monitoring of Sasrin-like Resin Bound Imines by Fluorescence Spectroscopy Domingo Madrigal Georgina Pina Luis Ignacio A. Rivero Multidisciplinaria (Ciencias Naturales y Exactas) solid phase monitoring reaction Fluorescence spectroscopy Merrifield resin was converted to various dialkyl-trihydroxybenzaldehyderesins and then to different bound imine resins.Fluorescence spectroscopy was used to continuously monitor theintermediates performed on the resins. Using fluorescent label (dansylchloride) information on the kinetics of the amine cleavage wasobtained. This study demonstrated that direct measures of fluorescenceintensity on single-resin beads can be an effective method ofmonitoring solid phase organic reactions 2006 artículo científico 1870-249X https://www.redalyc.org/articulo.oa?id=47550406 en http://www.redalyc.org/revista.oa?id=475 Journal of the Mexican Chemical Society application/pdf Sociedad Química de México Journal of the Mexican Chemical Society (México) Num.4 Vol.50 |
| format | Artículo científico |
| id | redalyc_47550406 |
| institution | Redalyc |
| language | en |
| publishDate | 2006 |
| publisher | Sociedad Química de México |
| spellingShingle | Synthesis and Hydrolysis Monitoring of Sasrin-like Resin Bound Imines by Fluorescence Spectroscopy Domingo Madrigal Multidisciplinaria (Ciencias Naturales y Exactas) solid phase monitoring reaction Fluorescence spectroscopy Synthesis and Hydrolysis Monitoring of Sasrin-like Resin Bound Imines by Fluorescence Spectroscopy Domingo Madrigal Georgina Pina Luis Ignacio A. Rivero Multidisciplinaria (Ciencias Naturales y Exactas) solid phase monitoring reaction Fluorescence spectroscopy Merrifield resin was converted to various dialkyl-trihydroxybenzaldehyderesins and then to different bound imine resins.Fluorescence spectroscopy was used to continuously monitor theintermediates performed on the resins. Using fluorescent label (dansylchloride) information on the kinetics of the amine cleavage wasobtained. This study demonstrated that direct measures of fluorescenceintensity on single-resin beads can be an effective method ofmonitoring solid phase organic reactions 2006 artículo científico 1870-249X https://www.redalyc.org/articulo.oa?id=47550406 en http://www.redalyc.org/revista.oa?id=475 Journal of the Mexican Chemical Society application/pdf Sociedad Química de México Journal of the Mexican Chemical Society (México) Num.4 Vol.50 |
| title | Synthesis and Hydrolysis Monitoring of Sasrin-like Resin Bound Imines by Fluorescence Spectroscopy |
| topic | Multidisciplinaria (Ciencias Naturales y Exactas) solid phase monitoring reaction Fluorescence spectroscopy |
| url | https://www.redalyc.org/articulo.oa?id=47550406 |