Fast and Green Methodto Synthesis of Quinolone Carboxylic Acid Derivatives Using Giant-Ball Nanoporous Isopolyoxomolybdate as Highly Efficient Recyclable Catalyst in Refluxing Water
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| Natura: | Artículo científico |
| Lingua: | en |
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Sociedad Química de México
2017
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| _version_ | 1876450821066981376 |
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| author | Yahya Mirzaie |
| author_facet | Yahya Mirzaie |
| contents | Fast and Green Methodto Synthesis of Quinolone Carboxylic Acid Derivatives Using Giant-Ball Nanoporous Isopolyoxomolybdate as Highly Efficient Recyclable Catalyst in Refluxing Water Yahya Mirzaie Jalil Lari Hooshang Vahedi Mohammad Hakimi Ahmad Nakhaei Abdolreza Rezaeifard Multidisciplinaria (Ciencias Naturales y Exactas) Keplerate {Mo 132 } fast and green synthesis Fluoroquinolone derivatives Various potentials antibacterial fluoroquinolone com - pounds were prepared by the direct amination of 7-halo-6- fluoro - quinolone-3-carboxylic acids with variety of piperazine derivatives and (4aR,7aR)-octahydro-1H-pyrrolo[3,4-b] pyridine using (NH 4 ) 42 [Mo VI 72 Mo V 60 O 372 (CH 3 COO) 30 (H 2 O) 72 ], a Keplerate-type giant-ball nanoporous isopolyoxomolybdate, as a catalyst in refluxing water. The results showed that this catalyst acts as effective catalyst and the reac - tion proceeded more easily and gave the highest yields of the products in short reaction time under refluxing water. Short reaction times, sim - ple isolation of the products, and usage of eco-friendly catalysts are some features of this procedure. In addition, the catalysts was easily recovered and used in multiple catalytic cycles. This material was pre - pared according to a previously published literature procedure using inexpensive and readily available starting materials. 2017 artículo científico 1870-249X https://www.redalyc.org/articulo.oa?id=47551118005 en http://www.redalyc.org/revista.oa?id=475 Journal of the Mexican Chemical Society application/pdf Sociedad Química de México Journal of the Mexican Chemical Society (México) Num.1 Vol.61 |
| format | Artículo científico |
| id | redalyc_47551118005 |
| institution | Redalyc |
| language | en |
| publishDate | 2017 |
| publisher | Sociedad Química de México |
| spellingShingle | Fast and Green Methodto Synthesis of Quinolone Carboxylic Acid Derivatives Using Giant-Ball Nanoporous Isopolyoxomolybdate as Highly Efficient Recyclable Catalyst in Refluxing Water Yahya Mirzaie Multidisciplinaria (Ciencias Naturales y Exactas) Keplerate {Mo 132 } fast and green synthesis Fluoroquinolone derivatives Fast and Green Methodto Synthesis of Quinolone Carboxylic Acid Derivatives Using Giant-Ball Nanoporous Isopolyoxomolybdate as Highly Efficient Recyclable Catalyst in Refluxing Water Yahya Mirzaie Jalil Lari Hooshang Vahedi Mohammad Hakimi Ahmad Nakhaei Abdolreza Rezaeifard Multidisciplinaria (Ciencias Naturales y Exactas) Keplerate {Mo 132 } fast and green synthesis Fluoroquinolone derivatives Various potentials antibacterial fluoroquinolone com - pounds were prepared by the direct amination of 7-halo-6- fluoro - quinolone-3-carboxylic acids with variety of piperazine derivatives and (4aR,7aR)-octahydro-1H-pyrrolo[3,4-b] pyridine using (NH 4 ) 42 [Mo VI 72 Mo V 60 O 372 (CH 3 COO) 30 (H 2 O) 72 ], a Keplerate-type giant-ball nanoporous isopolyoxomolybdate, as a catalyst in refluxing water. The results showed that this catalyst acts as effective catalyst and the reac - tion proceeded more easily and gave the highest yields of the products in short reaction time under refluxing water. Short reaction times, sim - ple isolation of the products, and usage of eco-friendly catalysts are some features of this procedure. In addition, the catalysts was easily recovered and used in multiple catalytic cycles. This material was pre - pared according to a previously published literature procedure using inexpensive and readily available starting materials. 2017 artículo científico 1870-249X https://www.redalyc.org/articulo.oa?id=47551118005 en http://www.redalyc.org/revista.oa?id=475 Journal of the Mexican Chemical Society application/pdf Sociedad Química de México Journal of the Mexican Chemical Society (México) Num.1 Vol.61 |
| title | Fast and Green Methodto Synthesis of Quinolone Carboxylic Acid Derivatives Using Giant-Ball Nanoporous Isopolyoxomolybdate as Highly Efficient Recyclable Catalyst in Refluxing Water |
| topic | Multidisciplinaria (Ciencias Naturales y Exactas) Keplerate {Mo 132 } fast and green synthesis Fluoroquinolone derivatives |
| url | https://www.redalyc.org/articulo.oa?id=47551118005 |