Quantification of lead using atomic absorption spectrometry in thermoformed and biodegradable flexible films made from cassava (Manihot esculenta crantz)
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| Format: | Artículo científico |
| Langue: | en |
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Universidad Nacional de Colombia
2018
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| _version_ | 1876475518177509376 |
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| author | Maite del Pilar Rada Mendoza |
| author_facet | Maite del Pilar Rada Mendoza |
| contents | Quantification of lead using atomic absorption spectrometry in thermoformed and biodegradable flexible films made from cassava (Manihot esculenta crantz) Maite del Pilar Rada Mendoza María del Mar Villamiel Guerra Olga Lucía Hoyos Saavedra Leidy Fernanda Alvira Ingeniería lead grafite furnace Biodegradable polymers cassava (Manihot esculenta crantz) Recently developed biopolymers can contain lead due to contamination from the origin of the material used to make them. A method for determining the presence of lead is proposed, using GF-AAS in thermoformed and biodegradable flexible films and flour and starch samples from Cassava. Acid digestion with reflux was optimized and the statistical quality parameters were standardized. The graphite furnace heating program was adjusted through pyrolysis and atomization curves. The working range was from 2.0 to 7.0 µg/L, with limits of detection and quantification of 0.618 and 1.853 µg/L, respectively. The precision was evaluated using intermediate precision and repeatability of the method, which showed standard deviations of less than 4.70% and 4.36%, respectively. The percentage of recovery ranged from 94.8% to 106.5%. The results obtained support the suitability of the method for determining the presence of lead. Lead concentrations were below 1 mg/Kg, indicating that these polymers can be used for food containers. 2018 artículo científico 0012-7353 https://www.redalyc.org/articulo.oa?id=49658894031 https://www.redalyc.org/journal/496/49658894031/ https://www.redalyc.org/journal/496/49658894031/html/ https://www.redalyc.org/journal/496/49658894031/49658894031.epub https://www.redalyc.org/journal/496/49658894031/movil 10.15446/dyna.v85n207.72347 en http://www.redalyc.org/revista.oa?id=496 Dyna application/pdf Universidad Nacional de Colombia Dyna (Colombia) Num.207 Vol.85 |
| format | Artículo científico |
| id | redalyc_49658894031 |
| institution | Redalyc |
| language | en |
| publishDate | 2018 |
| publisher | Universidad Nacional de Colombia |
| spellingShingle | Quantification of lead using atomic absorption spectrometry in thermoformed and biodegradable flexible films made from cassava (Manihot esculenta crantz) Maite del Pilar Rada Mendoza Ingeniería lead grafite furnace Biodegradable polymers cassava (Manihot esculenta crantz) Quantification of lead using atomic absorption spectrometry in thermoformed and biodegradable flexible films made from cassava (Manihot esculenta crantz) Maite del Pilar Rada Mendoza María del Mar Villamiel Guerra Olga Lucía Hoyos Saavedra Leidy Fernanda Alvira Ingeniería lead grafite furnace Biodegradable polymers cassava (Manihot esculenta crantz) Recently developed biopolymers can contain lead due to contamination from the origin of the material used to make them. A method for determining the presence of lead is proposed, using GF-AAS in thermoformed and biodegradable flexible films and flour and starch samples from Cassava. Acid digestion with reflux was optimized and the statistical quality parameters were standardized. The graphite furnace heating program was adjusted through pyrolysis and atomization curves. The working range was from 2.0 to 7.0 µg/L, with limits of detection and quantification of 0.618 and 1.853 µg/L, respectively. The precision was evaluated using intermediate precision and repeatability of the method, which showed standard deviations of less than 4.70% and 4.36%, respectively. The percentage of recovery ranged from 94.8% to 106.5%. The results obtained support the suitability of the method for determining the presence of lead. Lead concentrations were below 1 mg/Kg, indicating that these polymers can be used for food containers. 2018 artículo científico 0012-7353 https://www.redalyc.org/articulo.oa?id=49658894031 https://www.redalyc.org/journal/496/49658894031/ https://www.redalyc.org/journal/496/49658894031/html/ https://www.redalyc.org/journal/496/49658894031/49658894031.epub https://www.redalyc.org/journal/496/49658894031/movil 10.15446/dyna.v85n207.72347 en http://www.redalyc.org/revista.oa?id=496 Dyna application/pdf Universidad Nacional de Colombia Dyna (Colombia) Num.207 Vol.85 |
| title | Quantification of lead using atomic absorption spectrometry in thermoformed and biodegradable flexible films made from cassava (Manihot esculenta crantz) |
| topic | Ingeniería lead grafite furnace Biodegradable polymers cassava (Manihot esculenta crantz) |
| url | https://www.redalyc.org/articulo.oa?id=49658894031 https://www.redalyc.org/journal/496/49658894031/ https://www.redalyc.org/journal/496/49658894031/html/ https://www.redalyc.org/journal/496/49658894031/49658894031.epub https://www.redalyc.org/journal/496/49658894031/movil |