Glow discharge effect on temperature and time of treatment for the synthesis of Mo-doped manganite

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Autore principale: Iván Supelano-García
Natura: Artículo científico
Lingua:en
Pubblicazione: Universidad Nacional de Colombia 2019
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author Iván Supelano-García
author_facet Iván Supelano-García
contents Glow discharge effect on temperature and time of treatment for the synthesis of Mo-doped manganite Iván Supelano-García Willian Arnulfo Aperador-Chaparro Carlos Arturo Parra-Vargas Armando Sarmiento-Santos Ingeniería manganite Glow discharge magnetic properties structural properties We report the synthesis of CaMn0.9Mo0.1O3 manganite by glow discharge (GD) plasma treatment under Argon-Air atmosphere. The morphological, structural and magnetic properties were evaluated by scanning electron microscopy (SEM), X-ray diffraction (XRD) and magnetization measures. The results from these measures reveal that the properties of GD synthesized manganite are similar to that exhibited by CaMn0.9Mo0.1O3 produced by conventional resistive furnace. The Rietveld analysis of XRD patterns performed at room temperature show that the samples crystallize in orthorhombic structure of Pnma (62) space group. The magnetization curves as a function of temperature show two inflection points related to paramagnetic-antiferromagnetic and structural transition. The GD treatment produces a compound with similar properties, reducing the time and energy consumption in comparison with conventional synthesis route by using resistive furnace. 2019 artículo científico 0012-7353 https://www.redalyc.org/articulo.oa?id=49662418026 https://www.redalyc.org/journal/496/49662418026/ https://www.redalyc.org/journal/496/49662418026/html/ https://www.redalyc.org/journal/496/49662418026/49662418026.epub https://www.redalyc.org/journal/496/49662418026/movil 10.15446/dyna.v86n209.77832 en http://www.redalyc.org/revista.oa?id=496 Dyna application/pdf Universidad Nacional de Colombia Dyna (Colombia) Num.209 Vol.86
format Artículo científico
id redalyc_49662418026
institution Redalyc
language en
publishDate 2019
publisher Universidad Nacional de Colombia
spellingShingle Glow discharge effect on temperature and time of treatment for the synthesis of Mo-doped manganite
Iván Supelano-García
Ingeniería
manganite
Glow discharge
magnetic properties
structural properties
Glow discharge effect on temperature and time of treatment for the synthesis of Mo-doped manganite Iván Supelano-García Willian Arnulfo Aperador-Chaparro Carlos Arturo Parra-Vargas Armando Sarmiento-Santos Ingeniería manganite Glow discharge magnetic properties structural properties We report the synthesis of CaMn0.9Mo0.1O3 manganite by glow discharge (GD) plasma treatment under Argon-Air atmosphere. The morphological, structural and magnetic properties were evaluated by scanning electron microscopy (SEM), X-ray diffraction (XRD) and magnetization measures. The results from these measures reveal that the properties of GD synthesized manganite are similar to that exhibited by CaMn0.9Mo0.1O3 produced by conventional resistive furnace. The Rietveld analysis of XRD patterns performed at room temperature show that the samples crystallize in orthorhombic structure of Pnma (62) space group. The magnetization curves as a function of temperature show two inflection points related to paramagnetic-antiferromagnetic and structural transition. The GD treatment produces a compound with similar properties, reducing the time and energy consumption in comparison with conventional synthesis route by using resistive furnace. 2019 artículo científico 0012-7353 https://www.redalyc.org/articulo.oa?id=49662418026 https://www.redalyc.org/journal/496/49662418026/ https://www.redalyc.org/journal/496/49662418026/html/ https://www.redalyc.org/journal/496/49662418026/49662418026.epub https://www.redalyc.org/journal/496/49662418026/movil 10.15446/dyna.v86n209.77832 en http://www.redalyc.org/revista.oa?id=496 Dyna application/pdf Universidad Nacional de Colombia Dyna (Colombia) Num.209 Vol.86
title Glow discharge effect on temperature and time of treatment for the synthesis of Mo-doped manganite
topic Ingeniería
manganite
Glow discharge
magnetic properties
structural properties
url https://www.redalyc.org/articulo.oa?id=49662418026
https://www.redalyc.org/journal/496/49662418026/
https://www.redalyc.org/journal/496/49662418026/html/
https://www.redalyc.org/journal/496/49662418026/49662418026.epub
https://www.redalyc.org/journal/496/49662418026/movil