Synthesis of Thulium-yttria Nanoparticles with EPR Response

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Autor principal: S.C. Santos
Formato: Artículo científico
Lenguaje:en
Publicado: Sociedade Brasileira de Proteção Radiológica - SBPR 2022
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author S.C. Santos
author_facet S.C. Santos
contents Synthesis of Thulium-yttria Nanoparticles with EPR Response S.C. Santos O.Jr Rodrigues L.L. Campos Biología EPR Yttria thulium oxide ceramic processing radiation dosimetry Approaches to form new materials for radiation dosimetry are essential to enhance quality assurance and quality improvement practices based on radiation protection concept. The present work reports a hydrothermal synthesis based on a relative low temperature and pressure to form thulium-yttria nanoparticles with electron paramagnetic resonance response. Thulium-yttria nanoparticles were prepared and characterized by XRD, SEM, PCS, and EPR. According to results, the hydrothermal method provided thulium-yttria nanoparticles with cubic C-type structure, mean particle size (d50) less than 160nm, and EPR response. The EPR spectra of powders exhibited two resonance peaks p1 and p2 recorded at 350 and 160mT, respectively. The enhancement of the EPR response of yttria by the use of thulium as a dopant provide meaningful parameters to advance in the formation of new rare earth-based materials for radiation dosimetry. 2022 artículo científico 2319-0612 https://www.redalyc.org/articulo.oa?id=722280973006 en http://www.redalyc.org/revista.oa?id=7222 Brazilian Journal of Radiation Sciences application/pdf Sociedade Brasileira de Proteção Radiológica - SBPR Brazilian Journal of Radiation Sciences (Brasil) Num.2A Vol.10
format Artículo científico
id redalyc_722280973006
institution Redalyc
language en
publishDate 2022
publisher Sociedade Brasileira de Proteção Radiológica - SBPR
spellingShingle Synthesis of Thulium-yttria Nanoparticles with EPR Response
S.C. Santos
Biología
EPR
Yttria
thulium oxide
ceramic processing
radiation dosimetry
Synthesis of Thulium-yttria Nanoparticles with EPR Response S.C. Santos O.Jr Rodrigues L.L. Campos Biología EPR Yttria thulium oxide ceramic processing radiation dosimetry Approaches to form new materials for radiation dosimetry are essential to enhance quality assurance and quality improvement practices based on radiation protection concept. The present work reports a hydrothermal synthesis based on a relative low temperature and pressure to form thulium-yttria nanoparticles with electron paramagnetic resonance response. Thulium-yttria nanoparticles were prepared and characterized by XRD, SEM, PCS, and EPR. According to results, the hydrothermal method provided thulium-yttria nanoparticles with cubic C-type structure, mean particle size (d50) less than 160nm, and EPR response. The EPR spectra of powders exhibited two resonance peaks p1 and p2 recorded at 350 and 160mT, respectively. The enhancement of the EPR response of yttria by the use of thulium as a dopant provide meaningful parameters to advance in the formation of new rare earth-based materials for radiation dosimetry. 2022 artículo científico 2319-0612 https://www.redalyc.org/articulo.oa?id=722280973006 en http://www.redalyc.org/revista.oa?id=7222 Brazilian Journal of Radiation Sciences application/pdf Sociedade Brasileira de Proteção Radiológica - SBPR Brazilian Journal of Radiation Sciences (Brasil) Num.2A Vol.10
title Synthesis of Thulium-yttria Nanoparticles with EPR Response
topic Biología
EPR
Yttria
thulium oxide
ceramic processing
radiation dosimetry
url https://www.redalyc.org/articulo.oa?id=722280973006