Synthesis and characterization of NaSbO3 compound
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| Format: | Artículo científico |
| Language: | en |
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Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C.
2007
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| _version_ | 1876476206964015104 |
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| author | E. Ramírez-Meneses |
| author_facet | E. Ramírez-Meneses |
| contents | Synthesis and characterization of NaSbO3 compound E. Ramírez-Meneses R. Escamilla M. A. Domínguez-Crespo J. O. Flores-Flores A. B. Soto-Guzmán E. Chavira Física, Astronomía y Matemáticas Perovskites ray diffraction Chemical synthesis alkaline metal antimonates In this study we sintered NaSbO3 compound at 860 ºC from Na2CO3 and Sb2O3, detailed structural and microstructural of the compound were studied. Refinement of the X-ray diffraction (XRD) patterns by method of Rietveld indicate that the crystal structure of NaSbO3 belongs to the trigonal system with hexagonal symmetry, space group 3R(No.148), lattice parameters a = 5.2944(4) Å, c = 15.9469(8) Å and volume V = 387.124(0) Å3 with Z = 6. Scanning electron microscopy (SEM) analysis displayed that sintered samples at temperatures lower than 750 ºC have a favorable effect on the homogeneity of the samples. 2007 artículo científico 1665-3521 https://www.redalyc.org/articulo.oa?id=94220404 en http://www.redalyc.org/revista.oa?id=942 Superficies y vacío application/pdf Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C. Superficies y vacío (México) Num.4 Vol.20 |
| format | Artículo científico |
| id | redalyc_94220404 |
| institution | Redalyc |
| language | en |
| publishDate | 2007 |
| publisher | Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C. |
| spellingShingle | Synthesis and characterization of NaSbO3 compound E. Ramírez-Meneses Física, Astronomía y Matemáticas Perovskites ray diffraction Chemical synthesis alkaline metal antimonates Synthesis and characterization of NaSbO3 compound E. Ramírez-Meneses R. Escamilla M. A. Domínguez-Crespo J. O. Flores-Flores A. B. Soto-Guzmán E. Chavira Física, Astronomía y Matemáticas Perovskites ray diffraction Chemical synthesis alkaline metal antimonates In this study we sintered NaSbO3 compound at 860 ºC from Na2CO3 and Sb2O3, detailed structural and microstructural of the compound were studied. Refinement of the X-ray diffraction (XRD) patterns by method of Rietveld indicate that the crystal structure of NaSbO3 belongs to the trigonal system with hexagonal symmetry, space group 3R(No.148), lattice parameters a = 5.2944(4) Å, c = 15.9469(8) Å and volume V = 387.124(0) Å3 with Z = 6. Scanning electron microscopy (SEM) analysis displayed that sintered samples at temperatures lower than 750 ºC have a favorable effect on the homogeneity of the samples. 2007 artículo científico 1665-3521 https://www.redalyc.org/articulo.oa?id=94220404 en http://www.redalyc.org/revista.oa?id=942 Superficies y vacío application/pdf Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C. Superficies y vacío (México) Num.4 Vol.20 |
| title | Synthesis and characterization of NaSbO3 compound |
| topic | Física, Astronomía y Matemáticas Perovskites ray diffraction Chemical synthesis alkaline metal antimonates |
| url | https://www.redalyc.org/articulo.oa?id=94220404 |