Colloidal synthesis of CoAl2O4 nanoparticles using dodecylamine and their structural characterization

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Autore principale: O. Blanco
Natura: Artículo científico
Lingua:en
Pubblicazione: Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C. 2016
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author O. Blanco
author_facet O. Blanco
contents Colloidal synthesis of CoAl2O4 nanoparticles using dodecylamine and their structural characterization O. Blanco J.P. Morán-Lázaro V.M. Rodríguez-Betancourtt J. Reyes-Gómez A. Barrera Física, Astronomía y Matemáticas A mechanism of formation of colloidal particles was proposed by LaMer and Dinegar in order try to explain the variation of the concentration of the reagents with the time in the colloidal solution. According to the LaMer mechanism, if the concentration of the reagents is increased gradually then this could reach the super - saturation limit and consequently, a nucleation and growth process occurs. From this point of view, in this work the formation of CoAl 2 O 4 nanoparticles in the under - supersaturation limit can be partially explained by this mechanism. A non - aqueous colloidal method was formulated using the organic compound dodecylamine as a surfactant agent. By a variation of dodecylamine concentration two distinct morpholo gies for the CoAl 2 O 4 spinel phase were obtained. The thermal decomposition of the precursor mixture resulted in the formation of the blue CoAl 2 O 4 spinel phase at a temperature of 800 °C . 2016 artículo científico 1665-3521 https://www.redalyc.org/articulo.oa?id=94251122004 en http://www.redalyc.org/revista.oa?id=942 Superficies y vacío application/pdf Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C. Superficies y vacío (México) Num.3 Vol.29
format Artículo científico
id redalyc_94251122004
institution Redalyc
language en
publishDate 2016
publisher Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C.
spellingShingle Colloidal synthesis of CoAl2O4 nanoparticles using dodecylamine and their structural characterization
O. Blanco
Física, Astronomía y Matemáticas
Colloidal synthesis of CoAl2O4 nanoparticles using dodecylamine and their structural characterization O. Blanco J.P. Morán-Lázaro V.M. Rodríguez-Betancourtt J. Reyes-Gómez A. Barrera Física, Astronomía y Matemáticas A mechanism of formation of colloidal particles was proposed by LaMer and Dinegar in order try to explain the variation of the concentration of the reagents with the time in the colloidal solution. According to the LaMer mechanism, if the concentration of the reagents is increased gradually then this could reach the super - saturation limit and consequently, a nucleation and growth process occurs. From this point of view, in this work the formation of CoAl 2 O 4 nanoparticles in the under - supersaturation limit can be partially explained by this mechanism. A non - aqueous colloidal method was formulated using the organic compound dodecylamine as a surfactant agent. By a variation of dodecylamine concentration two distinct morpholo gies for the CoAl 2 O 4 spinel phase were obtained. The thermal decomposition of the precursor mixture resulted in the formation of the blue CoAl 2 O 4 spinel phase at a temperature of 800 °C . 2016 artículo científico 1665-3521 https://www.redalyc.org/articulo.oa?id=94251122004 en http://www.redalyc.org/revista.oa?id=942 Superficies y vacío application/pdf Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C. Superficies y vacío (México) Num.3 Vol.29
title Colloidal synthesis of CoAl2O4 nanoparticles using dodecylamine and their structural characterization
topic Física, Astronomía y Matemáticas
url https://www.redalyc.org/articulo.oa?id=94251122004