Effect of wettability on the void formation during liquid infusion into fibers

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Main Authors: Jared Turner, Daniel Lippert, Dongjin Seo, Matthew Grasinger, Andy George
Format: Artículo Open Access
Published: Wiley 2024
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author Jared Turner
Daniel Lippert
Dongjin Seo
Matthew Grasinger
Andy George
author_facet Jared Turner
Daniel Lippert
Dongjin Seo
Matthew Grasinger
Andy George
Jared Turner
Daniel Lippert
Dongjin Seo
Matthew Grasinger
Andy George
collection Wiley Open Access
contents Effect of wettability on the void formation during liquid infusion into fibers Jared Turner Daniel Lippert Dongjin Seo Matthew Grasinger Andy George Polymer Composites Abstract Liquid composite molding (LCM) is a promising option for low‐cost manufacturing of high‐performance composites compared to traditional prepreg‐autoclave methods. Void formation may be the most significant roadblock to such adaptation of LCM. In this article, the hypothesis that higher wettability, that is, lower contact angles of liquid on solids, would lead to lower void content for LCM is tested. First, a theory that calculates the energy required to form a bubble with varying contact angles is formulated by considering interfacial energy differences of a system with and without it. To experimentally prove this hypothesis, six different carbon fiber reinforcement samples were prepared each with a different fiber surface treatment. The wettability from the surface treatments was evaluated with contact angle measurements based on capillary rise between two fiber yarns. Void formation in situ during infusion was evaluated by a series of 1D infusion experiments using the same six surface modifications. Of the six samples, the reinforcements coated with fluorinated alkane and aminosilane showed the highest wettability and lowest void content, confirming that a lower contact angle can reduce the formation of voids during the infusion process. Highlights Higher wettability was correlated with less bubble (void) formation. Theoretical model and LCM experimental confirmation. Various surface modifications of carbon fibers tested. Potential application: enhancement of properties from LCM manufactured parts. 10.1002/pc.28811 http://onlinelibrary.wiley.com/termsAndConditions#am
doi_str_mv 10.1002/pc.28811
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institution Wiley Open Access
license_str_mv http://onlinelibrary.wiley.com/termsAndConditions#am
publishDate 2024
publisher Wiley
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spellingShingle Effect of wettability on the void formation during liquid infusion into fibers
Jared Turner
Daniel Lippert
Dongjin Seo
Matthew Grasinger
Andy George
Polymer Composites
Effect of wettability on the void formation during liquid infusion into fibers Jared Turner Daniel Lippert Dongjin Seo Matthew Grasinger Andy George Polymer Composites Abstract Liquid composite molding (LCM) is a promising option for low‐cost manufacturing of high‐performance composites compared to traditional prepreg‐autoclave methods. Void formation may be the most significant roadblock to such adaptation of LCM. In this article, the hypothesis that higher wettability, that is, lower contact angles of liquid on solids, would lead to lower void content for LCM is tested. First, a theory that calculates the energy required to form a bubble with varying contact angles is formulated by considering interfacial energy differences of a system with and without it. To experimentally prove this hypothesis, six different carbon fiber reinforcement samples were prepared each with a different fiber surface treatment. The wettability from the surface treatments was evaluated with contact angle measurements based on capillary rise between two fiber yarns. Void formation in situ during infusion was evaluated by a series of 1D infusion experiments using the same six surface modifications. Of the six samples, the reinforcements coated with fluorinated alkane and aminosilane showed the highest wettability and lowest void content, confirming that a lower contact angle can reduce the formation of voids during the infusion process. Highlights Higher wettability was correlated with less bubble (void) formation. Theoretical model and LCM experimental confirmation. Various surface modifications of carbon fibers tested. Potential application: enhancement of properties from LCM manufactured parts. 10.1002/pc.28811 http://onlinelibrary.wiley.com/termsAndConditions#am
title Effect of wettability on the void formation during liquid infusion into fibers
topic Polymer Composites
url https://4spepublications.onlinelibrary.wiley.com/doi/10.1002/pc.28811