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Autori principali: Henrique Luiz Berthault Moura, Marcelo Henrique Gehlen
Natura: Artículo Open Access
Pubblicazione: Wiley 2025
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Accesso online:https://onlinelibrary.wiley.com/doi/10.1111/php.14087
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author Henrique Luiz Berthault Moura
Marcelo Henrique Gehlen
author_facet Henrique Luiz Berthault Moura
Marcelo Henrique Gehlen
Henrique Luiz Berthault Moura
Marcelo Henrique Gehlen
collection Wiley Open Access
contents Modulation of the fluorescence of graphene oxide micro‐flakes with addition of peripheral benzimidazole group Henrique Luiz Berthault Moura Marcelo Henrique Gehlen Photochemistry and Photobiology AbstractGraphene oxide (GO) is peripherally modified with the addition of 4‐(1H‐benzimidazol‐2‐yl) benzaldehyde using a Debus–Radziszewski reaction with its ortho‐quinone groups. The GO content of ortho‐quinone is enhanced by the oxidation of catechol groups using molybdic acid in a Froehde reaction. Following a Knoevenagel condensation of the peripherally substituted benzimidazole with methyl cyanoacetate, a fluorescent intramolecular charge‐transfer (ICT) chromophore is introduced in the GO structure, forming a new fluorescent material called GO‐BI (graphene oxide with benzimidazole). Its micro‐flake particle has emission concentrated in its border, as revealed by confocal and total internal reflection fluorescence microscopy (TIRFM) images. The emission spectrum of the GO‐BI micro‐particle is centered on 525 nm and the fluorescence decay is biexponential, with two main components of 1.6 and 7.0 ns when excited at 473 nm. 10.1111/php.14087 http://creativecommons.org/licenses/by-nc-nd/4.0/
doi_str_mv 10.1111/php.14087
format Artículo Open Access
id wiley_oa_10_1111_php_14087
institution Wiley Open Access
license_str_mv http://creativecommons.org/licenses/by-nc-nd/4.0/
publishDate 2025
publisher Wiley
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spellingShingle Modulation of the fluorescence of graphene oxide micro‐flakes with addition of peripheral benzimidazole group
Henrique Luiz Berthault Moura
Marcelo Henrique Gehlen
Photochemistry and Photobiology
Modulation of the fluorescence of graphene oxide micro‐flakes with addition of peripheral benzimidazole group Henrique Luiz Berthault Moura Marcelo Henrique Gehlen Photochemistry and Photobiology AbstractGraphene oxide (GO) is peripherally modified with the addition of 4‐(1H‐benzimidazol‐2‐yl) benzaldehyde using a Debus–Radziszewski reaction with its ortho‐quinone groups. The GO content of ortho‐quinone is enhanced by the oxidation of catechol groups using molybdic acid in a Froehde reaction. Following a Knoevenagel condensation of the peripherally substituted benzimidazole with methyl cyanoacetate, a fluorescent intramolecular charge‐transfer (ICT) chromophore is introduced in the GO structure, forming a new fluorescent material called GO‐BI (graphene oxide with benzimidazole). Its micro‐flake particle has emission concentrated in its border, as revealed by confocal and total internal reflection fluorescence microscopy (TIRFM) images. The emission spectrum of the GO‐BI micro‐particle is centered on 525 nm and the fluorescence decay is biexponential, with two main components of 1.6 and 7.0 ns when excited at 473 nm. 10.1111/php.14087 http://creativecommons.org/licenses/by-nc-nd/4.0/
title Modulation of the fluorescence of graphene oxide micro‐flakes with addition of peripheral benzimidazole group
topic Photochemistry and Photobiology
url https://onlinelibrary.wiley.com/doi/10.1111/php.14087