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Main Authors: Muhammad Saleh Faryabi, Ali Akbari, Mahboobeh Zahedifar
Format: Artículo Open Access
Published: Wiley 2025
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Online Access:https://onlinelibrary.wiley.com/doi/10.1111/php.14111
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author Muhammad Saleh Faryabi
Ali Akbari
Mahboobeh Zahedifar
author_facet Muhammad Saleh Faryabi
Ali Akbari
Mahboobeh Zahedifar
Muhammad Saleh Faryabi
Ali Akbari
Mahboobeh Zahedifar
collection Wiley Open Access
contents Copper‐modified titanium dioxide nanoparticles as a highly efficient photocatalyst for the synthesis of furan‐3‐carboxylate derivatives Muhammad Saleh Faryabi Ali Akbari Mahboobeh Zahedifar Photochemistry and Photobiology Abstract A heterogeneous photocatalyst based on copper‐modified titanium dioxide nanoparticles has been prepared and characterized. Copper‐modified nano‐titanium dioxide (Nano‐TiO 2 @CuO) is an efficient photocatalyst for the synthesis of furan‐3‐carboxylate derivatives through a radical addition–polar cyclization of β ‐ketoester derivatives and allyl chloride under the irradiation of blue light. Copper‐modified titanium dioxide nanoparticles 20% which show titanium dioxide‐copper cooperativity show a significantly better performance with respect to turnover numbers (number of product molecules per catalyst molecule = efficiency). The Nano‐TiO 2 @CuO catalyst is stable and can be reused multiple times without a significant change in activity. The particle sizes varied in the range of 25–80 nm. High yields of product, environmentally friendly, cost‐effective method, and easy work‐up are advantages of the present method. All synthesized compounds were characterized by NMR and FT‐IR spectroscopy. 10.1111/php.14111 http://onlinelibrary.wiley.com/termsAndConditions#vor
doi_str_mv 10.1111/php.14111
format Artículo Open Access
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institution Wiley Open Access
license_str_mv http://onlinelibrary.wiley.com/termsAndConditions#vor
publishDate 2025
publisher Wiley
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spellingShingle Copper‐modified titanium dioxide nanoparticles as a highly efficient photocatalyst for the synthesis of furan‐3‐carboxylate derivatives
Muhammad Saleh Faryabi
Ali Akbari
Mahboobeh Zahedifar
Photochemistry and Photobiology
Copper‐modified titanium dioxide nanoparticles as a highly efficient photocatalyst for the synthesis of furan‐3‐carboxylate derivatives Muhammad Saleh Faryabi Ali Akbari Mahboobeh Zahedifar Photochemistry and Photobiology Abstract A heterogeneous photocatalyst based on copper‐modified titanium dioxide nanoparticles has been prepared and characterized. Copper‐modified nano‐titanium dioxide (Nano‐TiO 2 @CuO) is an efficient photocatalyst for the synthesis of furan‐3‐carboxylate derivatives through a radical addition–polar cyclization of β ‐ketoester derivatives and allyl chloride under the irradiation of blue light. Copper‐modified titanium dioxide nanoparticles 20% which show titanium dioxide‐copper cooperativity show a significantly better performance with respect to turnover numbers (number of product molecules per catalyst molecule = efficiency). The Nano‐TiO 2 @CuO catalyst is stable and can be reused multiple times without a significant change in activity. The particle sizes varied in the range of 25–80 nm. High yields of product, environmentally friendly, cost‐effective method, and easy work‐up are advantages of the present method. All synthesized compounds were characterized by NMR and FT‐IR spectroscopy. 10.1111/php.14111 http://onlinelibrary.wiley.com/termsAndConditions#vor
title Copper‐modified titanium dioxide nanoparticles as a highly efficient photocatalyst for the synthesis of furan‐3‐carboxylate derivatives
topic Photochemistry and Photobiology
url https://onlinelibrary.wiley.com/doi/10.1111/php.14111