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Main Authors: Gustavo Wander Streit, Rafael Bernardino Rodrigues da Silva Taques, Gabriela Fernandes Barreto, Fabiano Vargas Pereira, Gilson DeFreitas‐Silva, Thiago Teixeira Tasso
Format: Artículo Open Access
Published: Wiley 2025
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Online Access:https://onlinelibrary.wiley.com/doi/10.1111/php.14119
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author Gustavo Wander Streit
Rafael Bernardino Rodrigues da Silva Taques
Gabriela Fernandes Barreto
Fabiano Vargas Pereira
Gilson DeFreitas‐Silva
Thiago Teixeira Tasso
author_facet Gustavo Wander Streit
Rafael Bernardino Rodrigues da Silva Taques
Gabriela Fernandes Barreto
Fabiano Vargas Pereira
Gilson DeFreitas‐Silva
Thiago Teixeira Tasso
Gustavo Wander Streit
Rafael Bernardino Rodrigues da Silva Taques
Gabriela Fernandes Barreto
Fabiano Vargas Pereira
Gilson DeFreitas‐Silva
Thiago Teixeira Tasso
collection Wiley Open Access
contents Enhanced fluorescence emission or singlet oxygen production of cationic porphyrazines and porphyrins through combination with carbon dots Gustavo Wander Streit Rafael Bernardino Rodrigues da Silva Taques Gabriela Fernandes Barreto Fabiano Vargas Pereira Gilson DeFreitas‐Silva Thiago Teixeira Tasso Photochemistry and Photobiology AbstractA cationic porphyrin and porphyrazine with the 3‐ethylpyridyl substituent (H2P and H2Pz) and their respective zinc complexes (ZnP and ZnPz) were assembled to a carbon dot (CD) synthesized from citric acid and ammonium citrate. A titration was performed using a fluorescence spectrophotometer to determine the stoichiometric ratio at which the maximum interaction between the substances occurs, as well as the Stern–Volmer constant and intrinsic binding constant. The combination between CD and porphyrins or porphyrazines was confirmed using UV–VIS absorption spectroscopy, fluorescence emission, zeta potential, and Diffusion‐Ordered NMR Spectroscopy (DOSY). It was observed that after combination, there is a decline in the absorption of porphyrin derivatives, a variation in the emission of porphyrazines, a subtle increase in the zeta potential compared to the isolated CD particles, and a variation in the translational diffusion coefficient. It was also found that upon combination with the CD, changes in the photophysical properties of the macrocycles occur, for example, the fluorescence quantum yield of H2Pz increases from 0.81 ± 0.03% to 1.97 ± 0.05% while the singlet oxygen quantum yield of H2P increases ca. 70%. These results exemplify the capacity of CD to boost some properties of photosensitizers that are key for photodynamic therapy applications. 10.1111/php.14119 http://creativecommons.org/licenses/by/4.0/
doi_str_mv 10.1111/php.14119
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institution Wiley Open Access
license_str_mv http://creativecommons.org/licenses/by/4.0/
publishDate 2025
publisher Wiley
record_format wiley_oa
spellingShingle Enhanced fluorescence emission or singlet oxygen production of cationic porphyrazines and porphyrins through combination with carbon dots
Gustavo Wander Streit
Rafael Bernardino Rodrigues da Silva Taques
Gabriela Fernandes Barreto
Fabiano Vargas Pereira
Gilson DeFreitas‐Silva
Thiago Teixeira Tasso
Photochemistry and Photobiology
Enhanced fluorescence emission or singlet oxygen production of cationic porphyrazines and porphyrins through combination with carbon dots Gustavo Wander Streit Rafael Bernardino Rodrigues da Silva Taques Gabriela Fernandes Barreto Fabiano Vargas Pereira Gilson DeFreitas‐Silva Thiago Teixeira Tasso Photochemistry and Photobiology AbstractA cationic porphyrin and porphyrazine with the 3‐ethylpyridyl substituent (H2P and H2Pz) and their respective zinc complexes (ZnP and ZnPz) were assembled to a carbon dot (CD) synthesized from citric acid and ammonium citrate. A titration was performed using a fluorescence spectrophotometer to determine the stoichiometric ratio at which the maximum interaction between the substances occurs, as well as the Stern–Volmer constant and intrinsic binding constant. The combination between CD and porphyrins or porphyrazines was confirmed using UV–VIS absorption spectroscopy, fluorescence emission, zeta potential, and Diffusion‐Ordered NMR Spectroscopy (DOSY). It was observed that after combination, there is a decline in the absorption of porphyrin derivatives, a variation in the emission of porphyrazines, a subtle increase in the zeta potential compared to the isolated CD particles, and a variation in the translational diffusion coefficient. It was also found that upon combination with the CD, changes in the photophysical properties of the macrocycles occur, for example, the fluorescence quantum yield of H2Pz increases from 0.81 ± 0.03% to 1.97 ± 0.05% while the singlet oxygen quantum yield of H2P increases ca. 70%. These results exemplify the capacity of CD to boost some properties of photosensitizers that are key for photodynamic therapy applications. 10.1111/php.14119 http://creativecommons.org/licenses/by/4.0/
title Enhanced fluorescence emission or singlet oxygen production of cationic porphyrazines and porphyrins through combination with carbon dots
topic Photochemistry and Photobiology
url https://onlinelibrary.wiley.com/doi/10.1111/php.14119