Role of low molecular weight additives on the early-stages of magnesium carbonate mineralization

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Main Authors: Ruiz-Agudo, Encarnación, Huber, Lisa, Bonilla-Correa, Sarah, Santoro, Francesco, Ruiz-Agudo, Cristina, Rodriguez-Navarro, Carlos
Format: Recurso digital
Published: Zenodo 2024
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author Ruiz-Agudo, Encarnación
Huber, Lisa
Bonilla-Correa, Sarah
Santoro, Francesco
Ruiz-Agudo, Cristina
Rodriguez-Navarro, Carlos
author_facet Ruiz-Agudo, Encarnación
Huber, Lisa
Bonilla-Correa, Sarah
Santoro, Francesco
Ruiz-Agudo, Cristina
Rodriguez-Navarro, Carlos
contents <p><span>The early stages of MgCO<sub>3</sub> formation remain highly unexplored as compared to CaCO<sub>3</sub>. Recent studies have shown that MgCO<sub>3</sub> precipitation is non-classic and involves the formation of amorphous magnesium carbonate (AMC) prior to the stable carbonate phase. Here, the synthesis of AMC was carried out at constant alkaline pH using a potentiometric titration setup. We investigated the influence of sodium citrate and acetate, low molecular weight additives, on the nucleation, growth, and stability of AMC and its recrystallization, enabling tailored control over its formation for both environmental and engineering applications. These additives delay AMC nucleation and significantly impact its stability, and their presence in solution result in its recrystallization into less hydrated crystalline MgCO<sub>3</sub> phases</span></p>
format Recurso digital
id zenodo_https___doi_org_10_5281_zenodo_14772781
institution Zenodo
language
publishDate 2024
publisher Zenodo
record_format zenodo
spellingShingle Role of low molecular weight additives on the early-stages of magnesium carbonate mineralization
Ruiz-Agudo, Encarnación
Huber, Lisa
Bonilla-Correa, Sarah
Santoro, Francesco
Ruiz-Agudo, Cristina
Rodriguez-Navarro, Carlos
<p><span>The early stages of MgCO<sub>3</sub> formation remain highly unexplored as compared to CaCO<sub>3</sub>. Recent studies have shown that MgCO<sub>3</sub> precipitation is non-classic and involves the formation of amorphous magnesium carbonate (AMC) prior to the stable carbonate phase. Here, the synthesis of AMC was carried out at constant alkaline pH using a potentiometric titration setup. We investigated the influence of sodium citrate and acetate, low molecular weight additives, on the nucleation, growth, and stability of AMC and its recrystallization, enabling tailored control over its formation for both environmental and engineering applications. These additives delay AMC nucleation and significantly impact its stability, and their presence in solution result in its recrystallization into less hydrated crystalline MgCO<sub>3</sub> phases</span></p>
title Role of low molecular weight additives on the early-stages of magnesium carbonate mineralization
url https://doi.org/10.5281/zenodo.14772781