THE MECHANICAL PROPERTY CHANGE OF A NEWLY DEVELOPED EPOXY SYSTEM AT HIGH TEMPERATURE AND OXIDATIVE CONDITIONS

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Main Authors: Jae-Rock Lee, Soo-Jin Park, Yeung-Keun Kim
Format: Recurso digital
Published: Zenodo 1999
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author Jae-Rock Lee
Soo-Jin Park
Yeung-Keun Kim
author_facet Jae-Rock Lee
Soo-Jin Park
Yeung-Keun Kim
contents A newly developed cationic catalyst, N-Benzylpyrazinium hexafluoroantimonate (BPH) has been used to cure epoxies. The effect of the catalyst concentrations on the thermal and mechanical properties has been studied. The used catalyst concentrations are 0.5, 1, 2, 3 and 5wt.%. Two given maximum retention times, i.e., 1028 hours at 265�C and 8 hours at 300�C were studied in terms of the mechanical flexural and impact properties in the presence of different concentrations of BPH in air condition. The BPH cured epoxies showed excellent thermo-oxidative resistance. Their mechanical properties nearly remained intact for the short retention times less than 12 hours. The maximum weight losses were about 4.5wt.% at 300�C and 12wt.% at 265�C. At 265�C, the finally retained flexural and impact strengths were respectively more than 30% and 40% on the basis of their initial values after the very long retention time of 1028 hours for the adequate catalyst concentrations of 1 and 2 wt. %.
format Recurso digital
id zenodo_https___doi_org_10_5281_zenodo_15419444
institution Zenodo
language
publishDate 1999
publisher Zenodo
record_format zenodo
spellingShingle THE MECHANICAL PROPERTY CHANGE OF A NEWLY DEVELOPED EPOXY SYSTEM AT HIGH TEMPERATURE AND OXIDATIVE CONDITIONS
Jae-Rock Lee
Soo-Jin Park
Yeung-Keun Kim
A newly developed cationic catalyst, N-Benzylpyrazinium hexafluoroantimonate (BPH) has been used to cure epoxies. The effect of the catalyst concentrations on the thermal and mechanical properties has been studied. The used catalyst concentrations are 0.5, 1, 2, 3 and 5wt.%. Two given maximum retention times, i.e., 1028 hours at 265�C and 8 hours at 300�C were studied in terms of the mechanical flexural and impact properties in the presence of different concentrations of BPH in air condition. The BPH cured epoxies showed excellent thermo-oxidative resistance. Their mechanical properties nearly remained intact for the short retention times less than 12 hours. The maximum weight losses were about 4.5wt.% at 300�C and 12wt.% at 265�C. At 265�C, the finally retained flexural and impact strengths were respectively more than 30% and 40% on the basis of their initial values after the very long retention time of 1028 hours for the adequate catalyst concentrations of 1 and 2 wt. %.
title THE MECHANICAL PROPERTY CHANGE OF A NEWLY DEVELOPED EPOXY SYSTEM AT HIGH TEMPERATURE AND OXIDATIVE CONDITIONS
url https://doi.org/10.5281/zenodo.15419444