Tuning the Photophysical Properties of Flavins by Attaching an Aryl Moiety via Direct C–C Bond Coupling

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Main Authors: Čubiňák, Marek, Varma, Naisargi, Oeser, Petr, Pokluda, Adam, Pavlovska, Tetiana, Cibulka, Radek, Sikorski, Marek, tobrman, tomas, University of Chemistry and Technology, Adam Mickiewicz University in Poznań
Format: Recurso digital
Language:English
Published: Zenodo 2022
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author Čubiňák, Marek
Varma, Naisargi
Oeser, Petr
Pokluda, Adam
Pavlovska, Tetiana
Cibulka, Radek
Sikorski, Marek
tobrman, tomas
University of Chemistry and Technology
Adam Mickiewicz University in Poznań
author_facet Čubiňák, Marek
Varma, Naisargi
Oeser, Petr
Pokluda, Adam
Pavlovska, Tetiana
Cibulka, Radek
Sikorski, Marek
tobrman, tomas
University of Chemistry and Technology
Adam Mickiewicz University in Poznań
contents <p>Palladium-catalyzed Suzuki reactions of brominated flavin derivatives (5-deazaflavins, alloxazines, and isoalloxazines) with boronic acids or boronic acid esters that occur readily under mild conditions were shown to be an effective tool for the synthesis of a broad range of 7/8-arylflavins. In general, the introduction of an aryl/heteroaryl group by means of a direct C–C bond has been shown to be a promising approach to tuning the photophysical properties of flavin derivatives. The aryl substituents caused a bathochromic shift in the absorption spectra of up to 52 nm and prolonged the fluorescence lifetime by up to 1 order of magnitude. Moreover, arylation of flavin derivatives decreased their ability to generate singlet oxygen.</p>
format Recurso digital
id zenodo_https___doi_org_10_5281_zenodo_17937080
institution Zenodo
language eng
publishDate 2022
publisher Zenodo
record_format zenodo
spellingShingle Tuning the Photophysical Properties of Flavins by Attaching an Aryl Moiety via Direct C–C Bond Coupling
Čubiňák, Marek
Varma, Naisargi
Oeser, Petr
Pokluda, Adam
Pavlovska, Tetiana
Cibulka, Radek
Sikorski, Marek
tobrman, tomas
University of Chemistry and Technology
Adam Mickiewicz University in Poznań
<p>Palladium-catalyzed Suzuki reactions of brominated flavin derivatives (5-deazaflavins, alloxazines, and isoalloxazines) with boronic acids or boronic acid esters that occur readily under mild conditions were shown to be an effective tool for the synthesis of a broad range of 7/8-arylflavins. In general, the introduction of an aryl/heteroaryl group by means of a direct C–C bond has been shown to be a promising approach to tuning the photophysical properties of flavin derivatives. The aryl substituents caused a bathochromic shift in the absorption spectra of up to 52 nm and prolonged the fluorescence lifetime by up to 1 order of magnitude. Moreover, arylation of flavin derivatives decreased their ability to generate singlet oxygen.</p>
title Tuning the Photophysical Properties of Flavins by Attaching an Aryl Moiety via Direct C–C Bond Coupling
url https://doi.org/10.5281/zenodo.17937080