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2026
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| Online Access: | https://doi.org/10.5281/zenodo.19064181 |
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| author | Vesely, Martin |
| author_facet | Vesely, Martin |
| contents | <p>These dataset contain all raw material from the manuscript Rhodium on tungsten disulfide: catalyst design and optimization for styrene hydroformylation (ver 1.0)</p> <p> </p> <p><strong><span>Table 1. </span></strong><span>XRF results for catalysts supported on WS2</span></p> <p><strong><span>Fig. 2. </span></strong><span>XRD patterns of catalysts supported on WS2 with different Rh loading prepared by conventional wet impregnation at laboratory temperature with various metal loading.</span></p> <p><strong><span>Fig. 3. </span></strong><span>XRD patterns of catalysts supported on WS2 prepared at different impregnation temperatures (RT, 80 and 120 °C/reflux) and calcined at different temperatures (150, 300 and 450 °C)</span></p> <p><strong><span>Fig. 4. </span></strong><span>XRD patterns of Rh supported on pre-calcined WS2 prepared at different impregnation temperatures (RT, 80 and 120 °C/reflux) and one catalyst calcined at 300 °C</span></p> <p><strong><span>Fig. 5. </span></strong><span>SEM images of 2 wt% Rh/WS2 ((a) after impregnation and after calcination at (b) 150 °C, (c) 300 °C and at (d) 450 °C), of (e) 5 wt% Rh/WS2 and (f) 10 wt% Rh/WS2 after impregnation and of (g) pure pre-calcined WS2 and 2 wt% Rh/calc.WS2 ((h) after impregnation (at 120 °C/reflux) and (i) after calcination at 300 °C</span></p> <p><strong><span>Fig. 6. </span></strong><span>TEM images of 2 wt% Rh/WS2: (a) after impregnation and after calcination (b) at 150 °C, (c) at 300 °C, (d) at 450 °C, and (e) Rh particles size distributions and TEM image of 10 wt% Rh/WS2Rh (f) and its particles size distributions (g) and TEM images of 2 wt% Rh/calcined WS2 (120 °C/reflux): (h) after impregnation and (i) after calcination at 300 °C and their Rh particles size distributions (j)</span></p> <p><strong><span>Fig. 7. </span></strong><span>TEM/EDS elemental maps for Rh, W and S of 2 wt% Rh/WS2 calcined (a) at 150 °C, (b) at 300 °C (map of Rh, W and S)<strong> </strong></span></p> <p><strong><span>Fig. 8. </span></strong><span>Nitrogen adsorption-desorption isotherm comparison for (a) Rh/WS2 with increasing Rh loading and (b) Rh/WS2 catalysts calcined at different reaction temperature and (c) Rh supported on pre-calcined WS2</span></p> |
| format | Recurso digital |
| id | zenodo_https___doi_org_10_5281_zenodo_19064181 |
| institution | Zenodo |
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| publishDate | 2026 |
| publisher | Zenodo |
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| spellingShingle | Dataset for Rhodium on tungsten disulfide: catalyst design and optimization for styrene hydroformylation Vesely, Martin <p>These dataset contain all raw material from the manuscript Rhodium on tungsten disulfide: catalyst design and optimization for styrene hydroformylation (ver 1.0)</p> <p> </p> <p><strong><span>Table 1. </span></strong><span>XRF results for catalysts supported on WS2</span></p> <p><strong><span>Fig. 2. </span></strong><span>XRD patterns of catalysts supported on WS2 with different Rh loading prepared by conventional wet impregnation at laboratory temperature with various metal loading.</span></p> <p><strong><span>Fig. 3. </span></strong><span>XRD patterns of catalysts supported on WS2 prepared at different impregnation temperatures (RT, 80 and 120 °C/reflux) and calcined at different temperatures (150, 300 and 450 °C)</span></p> <p><strong><span>Fig. 4. </span></strong><span>XRD patterns of Rh supported on pre-calcined WS2 prepared at different impregnation temperatures (RT, 80 and 120 °C/reflux) and one catalyst calcined at 300 °C</span></p> <p><strong><span>Fig. 5. </span></strong><span>SEM images of 2 wt% Rh/WS2 ((a) after impregnation and after calcination at (b) 150 °C, (c) 300 °C and at (d) 450 °C), of (e) 5 wt% Rh/WS2 and (f) 10 wt% Rh/WS2 after impregnation and of (g) pure pre-calcined WS2 and 2 wt% Rh/calc.WS2 ((h) after impregnation (at 120 °C/reflux) and (i) after calcination at 300 °C</span></p> <p><strong><span>Fig. 6. </span></strong><span>TEM images of 2 wt% Rh/WS2: (a) after impregnation and after calcination (b) at 150 °C, (c) at 300 °C, (d) at 450 °C, and (e) Rh particles size distributions and TEM image of 10 wt% Rh/WS2Rh (f) and its particles size distributions (g) and TEM images of 2 wt% Rh/calcined WS2 (120 °C/reflux): (h) after impregnation and (i) after calcination at 300 °C and their Rh particles size distributions (j)</span></p> <p><strong><span>Fig. 7. </span></strong><span>TEM/EDS elemental maps for Rh, W and S of 2 wt% Rh/WS2 calcined (a) at 150 °C, (b) at 300 °C (map of Rh, W and S)<strong> </strong></span></p> <p><strong><span>Fig. 8. </span></strong><span>Nitrogen adsorption-desorption isotherm comparison for (a) Rh/WS2 with increasing Rh loading and (b) Rh/WS2 catalysts calcined at different reaction temperature and (c) Rh supported on pre-calcined WS2</span></p> |
| title | Dataset for Rhodium on tungsten disulfide: catalyst design and optimization for styrene hydroformylation |
| url | https://doi.org/10.5281/zenodo.19064181 |